C₁₇H₂₅NO₃

Base Information

• Chemical Name: C₁₇H₂₅NO₃
• CAS No.: 1075175-65-3
• Molecular Formula: C₁₇H₂₅NO₃
• Molecular Weight: 291.39
• Mol file: 1075175-65-3.mol

Synonyms:C₁₇H₂₅NO₃

Chemical Property of C₁₇H₂₅NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₅NO₃

There total 7 articles about C₁₇H₂₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyl azide → C17H25NO3 (1075175-65-3)

Guidance literature:

Multi-step reaction with 4 steps

1: methanesulfonamide; water / tert-butyl alcohol / 24 h / 0 °C

2: triphenylphosphine / tetrahydrofuran; water / 5 h / 50 °C

3: tetrabutylammonium acetate; palladium diacetate / 5 h / 90 °C / Inert atmosphere

4: potassium carbonate / methanol; water / 5 h / 50 °C

With methanesulfonamide; water; tetrabutylammonium acetate; palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; water; tert-butyl alcohol;

Reference yield:

ethyl 3-bromo-cinnamate (24398-80-9) → C17H25NO3 (1075175-65-3)

Guidance literature:

Multi-step reaction with 7 steps

1: diisobutylaluminium hydride / diethyl ether; dichloromethane / 0.5 h / 0 °C

2: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C

3: sodium azide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene / tetrahydrofuran; water; ethyl acetate / 4 h / 60 °C / Inert atmosphere

4: methanesulfonamide; water / tert-butyl alcohol / 24 h / 0 °C

5: triphenylphosphine / tetrahydrofuran; water / 5 h / 50 °C

6: tetrabutylammonium acetate; palladium diacetate / 5 h / 90 °C / Inert atmosphere

7: potassium carbonate / methanol; water / 5 h / 50 °C

With dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene; sodium azide; methanesulfonamide; water; tetrabutylammonium acetate; palladium diacetate; diisobutylaluminium hydride; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; tert-butyl alcohol;

Reference yield:

3-bromocinnamyl acetate (1149357-95-8) → C17H25NO3 (1075175-65-3)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium azide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene / tetrahydrofuran; water; ethyl acetate / 4 h / 60 °C / Inert atmosphere

2: methanesulfonamide; water / tert-butyl alcohol / 24 h / 0 °C

3: triphenylphosphine / tetrahydrofuran; water / 5 h / 50 °C

4: tetrabutylammonium acetate; palladium diacetate / 5 h / 90 °C / Inert atmosphere

5: potassium carbonate / methanol; water / 5 h / 50 °C

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene; sodium azide; methanesulfonamide; water; tetrabutylammonium acetate; palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; water; ethyl acetate; tert-butyl alcohol;

upstream raw materials:

ethyl 3-bromo-cinnamate

3-(m-Bromphenyl)-allylalkohol

3-bromocinnamyl acetate

m-bromobenzoic aldehyde