4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide

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Chemical Name:4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide
CAS No.:102670-65-5
Molecular Formula:C₁₈H₂₈ClN₃O₃
Molecular Weight:369.892
Hs Code.:

Synonyms:4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide

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Chemical Property of 4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide

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Technology Process of 4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide

There total 3 articles about 4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 38059-78-8
4-amino-5-chloro-N-<2-(diethylamino)ethyl>-2-hydroxybenzamide hydrochloride

: 19967-55-6
1-bromo-3-methyl-2-butanone

: 102670-65-5
4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield: 73.0%

: 38339-95-6
4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-hydroxybenzamide

: 19967-55-6
1-bromo-3-methyl-2-butanone

: 102670-65-5
4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 16h; Ambient temperature;
DOI:10.1021/jm00403a011

Reference yield:

: 364-62-5
metoclopramide

: 102670-65-5
4-Amino-5-chloro-N-[2-(diethylamino)ethyl]-2-[(3-methyl)-butan-2-on-1-yl]oxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / sodium hydride, ethanethiol / dimethylformamide / 1.5 h / 100 - 105 °C

2: 73 percent / sodium hydride / dimethylformamide / 16 h / Ambient temperature

With sodium hydride; ethanethiol; In N,N-dimethyl-formamide;
DOI:10.1021/jm00403a011