Technology Process of C40H51FN4O11
There total 18 articles about C40H51FN4O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / 1,4-dioxane; water / 15 h / 20 °C
2: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 h / 20 °C
With
1-hydroxy-7-aza-benzotriazole; sodium carbonate; N-ethyl-N,N-diisopropylamine; HATU;
In
1,4-dioxane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); 1,3-dimethylbarbituric acid / dichloromethane; ethyl acetate / 2 h / 20 °C
2: sodium carbonate / water; 1,4-dioxane / 15 h / 0 - 20 °C
3: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine
With
tetrakis(triphenylphosphine) palladium(0); 1-hydroxy-7-aza-benzotriazole; 1,3-dimethylbarbituric acid; sodium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,4-dioxane; dichloromethane; water; ethyl acetate;
