1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene

Base Information

Chemical Name:1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene
CAS No.:153227-11-3
Molecular Formula:C₃₂H₄₀N₂O₂
Molecular Weight:484.682
Hs Code.:

Synonyms:1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene

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Chemical Property of 1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene

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Technology Process of 1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene

There total 8 articles about 1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 28611-39-4
4-(dimethylamino)benzene-boronic acid

: 152120-06-4
1-bromo-2-benzyloxy-4-(6-methyl-6-cyanoheptyloxy)-5-ethylbenzene

: 153227-11-3
1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; benzene; for 16h; Heating;
DOI:10.1021/jm00022a006

Reference yield:

: 152609-39-7
4-(benzyloxy)-2-<(6-methyl-6-cyanoheptyl)oxy>acetophenone

: 153227-11-3
1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / trifluoroacetic acid, triethylsilane / CCl₄ / 1.5 h / Ambient temperature

2: 98 percent / N-bromosuccinimide / CCl₄ / 6 h / Ambient temperature

3: 94 percent / Pd(PPh₃)4, aq. Na₂CO₃ / ethanol; benzene / 16 h / Heating

With triethylsilane; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trifluoroacetic acid; In tetrachloromethane; ethanol; benzene;
DOI:10.1021/jm00022a006

Reference yield:

: 29682-12-0
1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone

: 153227-11-3
1-(benzyloxy)-2-<4-(dimethylamino)phenyl>-4-ethyl-5-<(6-methyl-6-cyanoheptyl)oxy>benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / K₂CO₃, KI / dimethylformamide / 24 h / 90 °C

2: 92 percent / trifluoroacetic acid, triethylsilane / CCl₄ / 1.5 h / Ambient temperature

3: 98 percent / N-bromosuccinimide / CCl₄ / 6 h / Ambient temperature

4: 94 percent / Pd(PPh₃)4, aq. Na₂CO₃ / ethanol; benzene / 16 h / Heating

With triethylsilane; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; trifluoroacetic acid; potassium iodide; In tetrachloromethane; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00022a006