(2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester

Base Information

Chemical Name:(2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester
CAS No.:194551-78-5
Molecular Formula:C₃₁H₄₃NO₃
Molecular Weight:477.687
Hs Code.:

Synonyms:(2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester

Chemical Property:

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Technology Process of (2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester

There total 3 articles about (2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-Cyclohexylmethyl-3-((S)-2-dibenzylamino-4-methyl-pentanoyl)-succinic acid 4-tert-butyl ester 1-methyl ester

: 194551-78-5
(2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 24h; Yield given; Ambient temperature;
DOI:10.1021/jo970579s

Reference yield:

: 194551-69-4
(S)-4-Dibenzylamino-6-methyl-3-oxo-heptanoic acid tert-butyl ester

: 194551-78-5
(2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1) THF, 0 deg C, 10 min; 2) THF, CH₂Cl₂, rt, 24 h

2: TFA / CH₂Cl₂ / 24 h / Ambient temperature

With sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo970579s

Reference yield:

: (S)-3-Cyclohexyl-2-trifluoromethanesulfonyloxy-propionic acid methyl ester

: 194551-78-5
(2S,5S)-2-Cyclohexylmethyl-5-dibenzylamino-7-methyl-4-oxo-octanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1) THF, 0 deg C, 10 min; 2) THF, CH₂Cl₂, rt, 24 h

2: TFA / CH₂Cl₂ / 24 h / Ambient temperature

With sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo970579s