6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime]

Base Information

• Chemical Name: 6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime]
• CAS No.: 228254-82-8
• Molecular Formula: C₅₅H₁₀₄N₂O₁₄Si₂
• Molecular Weight: 1073.61

Synonyms:6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime]

Chemical Property of 6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime]

Chemical Property:

Purity/Quality:

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Technology Process of 6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime]

There total 2 articles about 6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

allyl bromide (106-95-6) + E-2',4-O-bis(trimethylsilyl)erythromycin A 9-O-(1-isopropyloxycyclohexyl)oxime (206997-61-7) → 6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime] (228254-82-8)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.41667h; Inert atmosphere;

DOI:10.1021/jm100711p

Reference yield:

allyl bromide (106-95-6) + E-2',4-O-bis(trimethylsilyl)erythromycin A 9-O-(1-isopropyloxycyclohexyl)oxime (206997-61-7) → C58H108N2O14Si2 (1239612-90-8) + 6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime] (228254-82-8)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 5.41667h; Inert atmosphere;

DOI:10.1021/jm100711p

Reference yield:

6-O-allyl-2',4''-bis-O-trimethylsilylerythromycin A 9-[O-(1-isopropoxycyclohexyl)oxime] (228254-82-8) → C49H88N2O14

Guidance literature:

With acetic acid; In acetonitrile;

DOI:10.1016/S0960-894X(00)00106-2

upstream raw materials:

allyl bromide

E-2',4-O-bis(trimethylsilyl)erythromycin A 9-O-(1-isopropyloxycyclohexyl)oxime

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