3-benzyl-2-(4-methoxy-phenyl)-2H-indazole

Base Information

Chemical Name:3-benzyl-2-(4-methoxy-phenyl)-2H-indazole
CAS No.:1095510-29-4
Molecular Formula:C₂₁H₁₈N₂O
Molecular Weight:314.387
Hs Code.:

Synonyms:3-benzyl-2-(4-methoxy-phenyl)-2H-indazole

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Chemical Property of 3-benzyl-2-(4-methoxy-phenyl)-2H-indazole

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Technology Process of 3-benzyl-2-(4-methoxy-phenyl)-2H-indazole

There total 5 articles about 3-benzyl-2-(4-methoxy-phenyl)-2H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3682-75-5
2-(4-methoxyphenyl)-2H-indazole

: 108-88-3,15644-74-3,16713-13-6
toluene

: 1095510-29-4
3-benzyl-2-(4-methoxy-phenyl)-2H-indazole

Guidance literature:: With di-tert-butyl peroxide; tetra-(n-butyl)ammonium iodide; at 120 ℃; for 24h; Reagent/catalyst; Temperature; regioselective reaction; Catalytic behavior; Inert atmosphere; Sealed tube;
DOI:10.1039/d0ob01282c

Reference yield: 81.0%

: 10271-57-5
1-chloro-2-(2-phenylethynyl)benzene

: 19501-58-7
4-methoxyphenylhydrazine hydrochloride

: 1095510-29-4
3-benzyl-2-(4-methoxy-phenyl)-2H-indazole

Guidance literature:: With caesium carbonate; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate; In N,N-dimethyl-formamide; at 110 - 130 ℃; regioselective reaction;
DOI:10.1002/anie.200902323

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1095510-29-4
3-benzyl-2-(4-methoxy-phenyl)-2H-indazole

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 6 h / 60 °C / Inert atmosphere

2: copper(l) iodide; sodium azide; N,N,N,N,-tetramethylethylenediamine / dimethyl sulfoxide / 12 h / 120 °C / Inert atmosphere

3: tetra-(n-butyl)ammonium iodide; di-tert-butyl peroxide / 24 h / 120 °C / Inert atmosphere; Sealed tube

With copper(l) iodide; sodium azide; N,N,N,N,-tetramethylethylenediamine; di-tert-butyl peroxide; tetra-(n-butyl)ammonium iodide; In methanol; dimethyl sulfoxide;
DOI:10.1039/d0ob01282c