2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide

Base Information

Chemical Name:2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide
CAS No.:950588-84-8
Molecular Formula:C₁₃H₁₆FNO₂
Molecular Weight:237.274
Hs Code.:

Synonyms:2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide

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Chemical Property of 2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide

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Technology Process of 2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide

There total 2 articles about 2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 3-(3-fluoro-4-methyl-phenyl)-N-methoxy-N-methyl-acrylamide

: 1774-47-6
trimethylsulfoxonium iodide

: 950588-84-8
2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.75h;

Reference yield:

: 694511-55-2
(E)-3-(3-fluoro-4-methylphenyl)acrylic acid

: 950588-84-8
2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 48 h

2: sodium hydride / N,N-dimethyl-formamide / 2.75 h / 0 - 20 °C

With dmap; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield: 100.0%

: 950588-84-8
2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide

: 950588-85-9
2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid

Guidance literature:: 2-(3-fluoro-4-methyl-phenyl)-cyclopropanecarboxylic acid methoxy-methyl-amide; With sodium hydroxide; water; In methanol; for 3h; Heating / reflux;

With hydrogenchloride; In water;