methyl 15-(3-nitrophenyl)pentadec-12-enoate

Base Information

Chemical Name:methyl 15-(3-nitrophenyl)pentadec-12-enoate
CAS No.:121269-67-8
Molecular Formula:C₂₂H₃₃NO₄
Molecular Weight:375.508
Hs Code.:

Synonyms:methyl 15-(3-nitrophenyl)pentadec-12-enoate

Suppliers and Price of methyl 15-(3-nitrophenyl)pentadec-12-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 15-(3-nitrophenyl)pentadec-12-enoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 15-(3-nitrophenyl)pentadec-12-enoate

There total 8 articles about methyl 15-(3-nitrophenyl)pentadec-12-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 2009-59-8
methyl 11-formylundecanoate

: 121269-66-7
<3-(3-nitrophenyl)propyl>triphenylphosphonium bromide

: 121269-67-8
methyl 15-(3-nitrophenyl)pentadec-12-enoate

Guidance literature:: With potassium tert-butylate; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jm00129a014

Reference yield:

: 947-05-7
oxacyclotridecan-2-one

: 121269-67-8
methyl 15-(3-nitrophenyl)pentadec-12-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / 6 h / Heating

2: 68 percent / pyridinium chlorochromate (PCC) / CH₂Cl₂ / 2 h / Ambient temperature

3: 48 percent / KOt-Bu / CH₂Cl₂ / 3 h / Ambient temperature

With sulfuric acid; potassium tert-butylate; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/jm00129a014

Reference yield:

: 555-68-0,1772-76-5
m-Nitrocinnamic Acid

: 121269-67-8
methyl 15-(3-nitrophenyl)pentadec-12-enoate

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / (H₂NOH)2, H₂SO₄, H₂NOSO₃H, NaOH / H₂O / 5.5 h / 10 °C / pH 6-7

2: 72 percent / BF₃ / tetrahydrofuran / 2 h / Ambient temperature

3: 58 percent / PBr₃, pyridine / benzene / 1) 0 deg C, 1 h, 2) 65 deg C, 5.5 h

4: 66 percent / acetonitrile / 44 h / Heating

5: 48 percent / KOt-Bu / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; sodium hydroxide; (H₂NOH)2; sulfuric acid; boron trifluoride; potassium tert-butylate; phosphorus tribromide; hydroxylamine-O-sulfonic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/jm00129a014