alpha-D-Xylofuranuronicacid,3-amino-3-deoxy-1,2-O-(1-methylethylidene)-,methylester(9CI)

Base Information

Chemical Name:alpha-D-Xylofuranuronicacid,3-amino-3-deoxy-1,2-O-(1-methylethylidene)-,methylester(9CI)
CAS No.:800379-24-2
Molecular Formula:C9H15 N O5
Molecular Weight:217.22
Hs Code.:
Mol file:800379-24-2.mol

Synonyms:alpha-D-Xylofuranuronicacid,3-amino-3-deoxy-1,2-O-(1-methylethylidene)-,methylester(9CI)

Suppliers and Price of alpha-D-Xylofuranuronicacid,3-amino-3-deoxy-1,2-O-(1-methylethylidene)-,methylester(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of alpha-D-Xylofuranuronicacid,3-amino-3-deoxy-1,2-O-(1-methylethylidene)-,methylester(9CI)

Chemical Property:

Boiling Point:275.1±40.0 °C(Predicted)
PKA:6.43±0.60(Predicted)
PSA：80.01000
Density:1.208±0.06 g/cm3(Predicted)
LogP:0.06340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of alpha-D-Xylofuranuronicacid,3-amino-3-deoxy-1,2-O-(1-methylethylidene)-,methylester(9CI)

There total 5 articles about alpha-D-Xylofuranuronicacid,3-amino-3-deoxy-1,2-O-(1-methylethylidene)-,methylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1060716-74-6
methyl 3-azido-3-deoxy-1,2-O-(1-methylethylidne)-α-D-xylofuranoate

: 800379-24-2
methyl 3-amino-3-deoxy-1,2-O-(1-methylethylidne)-α-D-xylofuranoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/ja0467667

Reference yield:

: 13964-23-3
3-azido-3-deoxy-1,2:5,6-di-(O-isopropylidene)-α-D-glucofuranose

: 800379-24-2
methyl 3-amino-3-deoxy-1,2-O-(1-methylethylidne)-α-D-xylofuranoate

Guidance literature:: Multi-step reaction with 4 steps

1: mild acid hydrolysis

2: NaIO₄; NaClO₂; aq. H₂O₂ / NaH₂PO₄ / acetonitrile / 0 °C

3: diethyl ether / 0 °C

4: H₂ / Pd/C / ethyl acetate

With sodium chlorite; sodium periodate; hydrogen; dihydrogen peroxide; sodium dihydrogenphosphate; palladium on activated charcoal; In diethyl ether; ethyl acetate; acetonitrile;
DOI:10.1021/ja0467667

Reference yield:

: 22169-71-7
(R)-1-((3aR,5S,6S,6aR)-6-azido-2,2-dimethyltetrahydrofuro-[2,3-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 800379-24-2
methyl 3-amino-3-deoxy-1,2-O-(1-methylethylidne)-α-D-xylofuranoate

Guidance literature:: Multi-step reaction with 3 steps

1: NaIO₄; NaClO₂; aq. H₂O₂ / NaH₂PO₄ / acetonitrile / 0 °C

2: diethyl ether / 0 °C

3: H₂ / Pd/C / ethyl acetate

With sodium chlorite; sodium periodate; hydrogen; dihydrogen peroxide; sodium dihydrogenphosphate; palladium on activated charcoal; In diethyl ether; ethyl acetate; acetonitrile;
DOI:10.1021/ja0467667