(1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(R)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester]

Base Information

Chemical Name:(1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(R)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester]
CAS No.:883143-26-8
Molecular Formula:C₄₇H₅₁NO₈
Molecular Weight:757.924
Hs Code.:

Synonyms:(1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(R)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(R)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester]

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Technology Process of (1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(R)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester]

There total 1 articles about (1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(R)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 883143-21-3
methyl (2S)-benzylamino-2-(1-allyl-2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-ethanoate

: 883143-26-8
(1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(R)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester]

: (1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(S)-hydroxymethylene-spiro[1,5-anhydro-D-glucitol-1,3'-L-proline methyl ester]

: (1S)-2,3,4,6-tetra-O-benzyl-1'-N-benzyl-5'(S)-hydroxy-spiro[1,5-anhydro-D-glucitol-1,3'-L-pipecolic methyl ester]

Guidance literature:: methyl (2S)-benzylamino-2-(1-allyl-2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-ethanoate; With iodine; In diethyl ether; dichloromethane; at 0 - 20 ℃;

With silver(I) acetate; In toluene; at 20 ℃;

With potassium carbonate; In methanol; at 20 ℃; for 1h;
DOI:10.1016/j.carres.2008.12.024