dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)

Base Information

Chemical Name:dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)
CAS No.:1394350-82-3
Molecular Formula:C₂₂H₂₃I₂NO₆
Molecular Weight:651.237
Hs Code.:

Synonyms:dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)

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Chemical Property of dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)

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Technology Process of dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)

There total 2 articles about dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394351-52-0
C₂₃H₂₁I₂NO₆

: 1394350-82-3
dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)

Guidance literature:: With hydrogenchloride; water; In ethanol; at 20 ℃;
DOI:10.1021/ja306631z

Reference yield:

: 229028-10-8
methyl 4-(bromomethyl)-3-iodo-benzoate

: 1394350-82-3
dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / acetonitrile / 0 - 70 °C

2: water; hydrogenchloride / ethanol / 20 °C

With hydrogenchloride; water; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In ethanol; acetonitrile;
DOI:10.1021/ja306631z

Reference yield: 86.0%

: 1394350-82-3
dimethyl 4,4'-(2-amino-2-(ethoxycarbonyl)propane-1,3-diyl)-bis(3-iodobenzoate)

: 1394351-12-2
(S)-2-ethyl 6-methyl 2-(2-iodo-4-(methoxycarbonyl)benzyl)indoline-2,6-dicarboxylate

Guidance literature:: With copper(l) iodide; (Ra)-3,3’-di(anthracen-9-yl)-[1,1’-binaphthalene]-2,2’-diol; caesium carbonate; In 1,4-dioxane; at 20 ℃; for 10h; enantioselective reaction;
DOI:10.1021/ja306631z