[(η5-C5H5)2Zr(CH3)(CH2CMe3)]

Base Information

Chemical Name:[(η5-C5H5)2Zr(CH3)(CH2CMe3)]
CAS No.:177431-11-7
Molecular Formula:C₁₆H₂₄Zr
Molecular Weight:307.591
Hs Code.:

Synonyms:[(η5-C5H5)2Zr(CH3)(CH2CMe3)]

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Chemical Property of [(η5-C5H5)2Zr(CH3)(CH2CMe3)]

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Technology Process of [(η5-C5H5)2Zr(CH3)(CH2CMe3)]

There total 1 articles about [(η5-C5H5)2Zr(CH3)(CH2CMe3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: zirconocene methyl chloride

: 7412-67-1
neopentyl lithium

: 177431-11-7
[(η5-C5H5)2Zr(CH3)(CH2CMe3)]

Guidance literature:: In tetrahydrofuran; (Ar); THF added to a mixt. of Zr complex and Li compd. at -78°C, stirred for minutes at -78°C, allowed to warm to room temp.; solvent-removed, recrystd. (hexanes);
DOI:10.1021/om0504710

Reference yield:

: 177431-11-7
[(η5-C5H5)2Zr(CH3)(CH2CMe3)]

: 1109-15-5
tris(pentafluorophenyl)borate

: Cp2Zr(neopentyl)(μ-Me)B(C6F5)3

Guidance literature:: In further solvent(s); a soln. of Zr complex in C6D5Cl added slowly to B(C6F5)3 in C6D5Cl at -40°C; not isolated, detected by NMR;
DOI:10.1021/om0504710