9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine

Base Information

Chemical Name:9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine
CAS No.:525596-22-9
Molecular Formula:C₃₃H₂₉N₅O₇
Molecular Weight:607.623
Hs Code.:

Synonyms:9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine

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Technology Process of 9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine

There total 6 articles about 9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 525596-21-8
1,2-di-O-acetyl-5-O-benzoyl-3-O-benzyl-L-arabinofuranose

: 4005-49-6
N-benzoyladenine

: 525596-22-9
9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine

Guidance literature:: With tin(IV) chloride; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1016/j.tet.2005.12.007

Reference yield:

: 110237-79-1
5-O-benzoyl-3-O-benzyl-1,2-O-isopropylidene-β-L-arabinofuranose

: 525596-22-9
9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; aq. AcOH / 1 h / 50 °C

1.2: 73 percent / pyridine / 6 h / 50 °C

2.1: 88 percent / SnCl₄ / acetonitrile / 4 h / 20 °C

With sulfuric acid; tin(IV) chloride; acetic acid; In acetonitrile;
DOI:10.1016/j.tet.2005.12.007

Reference yield:

: 68354-70-1
3-O-benzyl-1,2-O-isopropylidene-β-L-arabinofuranose

: 525596-22-9
9-(2-O-acetyl-5-O-benzoyl-3-O-benzyl-α-L-arabinofuranosyl)-6-N-benzoyladenine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 74 percent / pyridine / 2 h / 20 °C

2.1: sulfuric acid; aq. AcOH / 1 h / 50 °C

2.2: 73 percent / pyridine / 6 h / 50 °C

3.1: 88 percent / SnCl₄ / acetonitrile / 4 h / 20 °C

With pyridine; sulfuric acid; tin(IV) chloride; acetic acid; In acetonitrile;
DOI:10.1016/j.tet.2005.12.007