C₂₈H₃₇F₂N₆O₈P

Base Information

Chemical Name:C₂₈H₃₇F₂N₆O₈P
CAS No.:1613589-85-7
Molecular Formula:C₂₈H₃₇F₂N₆O₈P
Molecular Weight:654.608
Hs Code.:

C<sub>28</sub>H<sub>37</sub>F<sub>2</sub>N<sub>6</sub>O<sub>8</sub>P

Synonyms:C₂₈H₃₇F₂N₆O₈P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₇F₂N₆O₈P

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Technology Process of C₂₈H₃₇F₂N₆O₈P

There total 16 articles about C₂₈H₃₇F₂N₆O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₈H₆₉F₂N₆O₁₀P

: 1613589-85-7
C₂₈H₃₇F₂N₆O₈P

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; acetonitrile; at 0 - 20 ℃; for 1h;

Reference yield:

: 1613589-70-0
9-(2,5-dideoxy-2-fluoro-2-C-methyl-5-iodo-β-D-ribofuranosyl)-6-ethoxy-2-((4-monomethoxytrityl)amino)purine

: 1613589-85-7
C₂₈H₃₇F₂N₆O₈P

Guidance literature:: Multi-step reaction with 7 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 3 h / Reflux

2: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 0 - 20 °C

3: silver nitrate / dichloromethane / 0 - 20 °C

4: 15-crown-5 / N,N-dimethyl-formamide / 72 h / 95 °C

5: ammonia / methanol / 18 h / 20 °C

6: 1-methyl-1H-imidazole / acetonitrile / 4 h / 0 - 5 °C

7: hydrogenchloride / 1,4-dioxane; acetonitrile / 1 h / 0 - 20 °C

With 1-methyl-1H-imidazole; hydrogenchloride; N-iodo-succinimide; 15-crown-5; ammonia; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1613589-69-7
9-(2-deoxy-2-fluoro-2-C-methyl-β-D-ribofuranosyl)-6-ethoxy-2-((4-monomethoxytrityl)amino)purine

: 1613589-85-7
C₂₈H₃₇F₂N₆O₈P

Guidance literature:: Multi-step reaction with 8 steps

1: triphenylphosphine; pyridine; iodine / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 3 h / Reflux

3: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 0 - 20 °C

4: silver nitrate / dichloromethane / 0 - 20 °C

5: 15-crown-5 / N,N-dimethyl-formamide / 72 h / 95 °C

6: ammonia / methanol / 18 h / 20 °C

7: 1-methyl-1H-imidazole / acetonitrile / 4 h / 0 - 5 °C

8: hydrogenchloride / 1,4-dioxane; acetonitrile / 1 h / 0 - 20 °C

With pyridine; 1-methyl-1H-imidazole; hydrogenchloride; N-iodo-succinimide; 15-crown-5; ammonia; iodine; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;