C₁₂H₁₂FN₃O₂S

Base Information

Chemical Name:C₁₂H₁₂FN₃O₂S
CAS No.:1200496-68-9
Molecular Formula:C₁₂H₁₂FN₃O₂S
Molecular Weight:281.311
Hs Code.:

C<sub>12</sub>H<sub>12</sub>FN<sub>3</sub>O<sub>2</sub>S

Synonyms:C₁₂H₁₂FN₃O₂S

Suppliers and Price of C₁₂H₁₂FN₃O₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₂FN₃O₂S

Chemical Property:

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Technology Process of C₁₂H₁₂FN₃O₂S

There total 8 articles about C₁₂H₁₂FN₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₁₆FN₃O₃S

: 1200496-68-9
C₁₂H₁₂FN₃O₂S

Guidance literature:: With hydrazine hydrate; In ethanol; at 50 ℃; for 2h;

Reference yield:

: 1075230-65-7
(S)-3-amino-3-(2-fluoro-5-nitrophenyl)butan-1-ol

: 1200496-68-9
C₁₂H₁₂FN₃O₂S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydrogencarbonate / water; tetrahydrofuran / 2.5 h / 20 °C

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C

3.1: titanium tetrachloride / diethyl ether / -78 - -40 °C

3.2: 3 h / -40 °C

3.3: 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 48 h / 20 °C

5.1: piperidine / N,N-dimethyl-formamide / 0.33 h / 20 °C

6.1: acetone / 0.33 h / 0 °C

7.1: sulfuric acid / 3 h / 20 °C

7.2: Cooling with ice

8.1: hydrazine hydrate / ethanol / 2 h / 50 °C

With piperidine; sulfuric acid; titanium tetrachloride; sodium hydrogencarbonate; hydrazine hydrate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1200496-60-1
C₂₅H₂₁FN₂O₅

: 1200496-68-9
C₁₂H₁₂FN₃O₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: titanium tetrachloride / diethyl ether / -78 - -40 °C

1.2: 3 h / -40 °C

1.3: 20 °C

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 48 h / 20 °C

3.1: piperidine / N,N-dimethyl-formamide / 0.33 h / 20 °C

4.1: acetone / 0.33 h / 0 °C

5.1: sulfuric acid / 3 h / 20 °C

5.2: Cooling with ice

6.1: hydrazine hydrate / ethanol / 2 h / 50 °C

With piperidine; sulfuric acid; titanium tetrachloride; hydrazine hydrate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In diethyl ether; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;