(5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester

Base Information

Chemical Name:(5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester
CAS No.:169701-56-8
Molecular Formula:C₂₇H₃₄N₂O₆
Molecular Weight:482.577
Hs Code.:

Synonyms:(5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester

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Technology Process of (5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester

There total 5 articles about (5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 68709-76-2
5(S)-<(butyloxycarbonyl)amino>-6-phenyl-4-oxohexanoic acid

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 169701-56-8
(5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/j.bmcl.2006.06.003

Reference yield: 95.0%

: 169701-56-8
(5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester

Guidance literature:

Reference yield: 44.0%

: (S)-2-((S)-3-Benzenesulfonyl-5-tert-butoxycarbonylamino-4-oxo-6-phenyl-hexanoylamino)-3-phenyl-propionic acid methyl ester

: 169701-56-8
(5S)-6-phenyl-5-[(tert-butyloxycarbonyl)amino]-4-oxo-hexanoyl-L-phenylalanine methyl ester

Guidance literature:: With samarium diiodide; In tetrahydrofuran; methanol; at -78 ℃; for 20h; to room temperature;
DOI:10.1016/0040-4039(95)00564-S