2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine

Base Information

Chemical Name:2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine
CAS No.:512785-68-1
Molecular Formula:C₆₁H₅₇NP₄
Molecular Weight:928.025
Hs Code.:

Synonyms:2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine

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Chemical Property of 2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine

Chemical Property:

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Technology Process of 2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine

There total 2 articles about 2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 512785-66-9
2,6-bis(2-bromo-1-bromomethyl-1-methylethyl)pyridine

: 512785-68-1
2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine

Guidance literature:: In tetrahydrofuran; for 12h; Heating;
DOI:10.1515/znb-2002-1110

Reference yield:

: C₄₁H₄₅NO₁₂S₄

: 512785-68-1
2,6-bis{2-(diphenylphosphanyl)-1-[(diphenylphosphanyl)methyl]-1-methylethyl}pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / LiBr / dimethylsulfoxide / 72 h / 70 °C

2: 65 percent / tetrahydrofuran / 12 h / Heating

With lithium bromide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1515/znb-2002-1110