7-iodo-1H-indole

Base Information

Chemical Name:7-iodo-1H-indole
CAS No.:89976-15-8
Molecular Formula:C8H6IN
Molecular Weight:243.047
Hs Code.:
European Community (EC) Number:625-422-8
DSSTox Substance ID:DTXSID00453092
Nikkaji Number:J782.401G
Wikidata:Q82274089
Mol file:89976-15-8.mol

Synonyms:7-iodo-1H-indole;89976-15-8;7-IODOINDOLE;7-Iodoindole, 97%;SCHEMBL3334473;DTXSID00453092;VBKAPLYISDSUCE-UHFFFAOYSA-N;MFCD10000889;AS-43817;CS-0188466

Suppliers and Price of 7-iodo-1H-indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
7-Iodoindole 97%
1g
$ 107.00

Crysdot
7-Iodo-1H-indole 95+%
1g
$ 560.00

Chemenu
7-iodo-1H-indole 95%
5g
$ 617.00

American Custom Chemicals Corporation
7-IODOINDOLE 95.00%
1G
$ 708.25

Ambeed
7-Iodo-1H-indole 95%
1g
$ 239.00

Ambeed
7-Iodo-1H-indole 95%
250mg
$ 90.00

Ambeed
7-Iodo-1H-indole 95%
5g
$ 788.00

Alichem
7-Iodo-1H-indole
10g
$ 1380.20

Total 16 raw suppliers

Chemical Property of 7-iodo-1H-indole

Chemical Property:

Melting Point:52-56 °C
Boiling Point:341.705 °C at 760 mmHg
Flash Point:160.458 °C
PSA：15.79000
Density:1.961 g/cm³
LogP:2.77250
Storage Temp.:2-8°C(protect from light)
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:242.95450
Heavy Atom Count:10
Complexity:126

Purity/Quality:

99% ^*data from raw suppliers

7-Iodoindole 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22-41
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C(=C1)I)NC=C2

Technology Process of 7-iodo-1H-indole

There total 12 articles about 7-iodo-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104682-96-4
2,3-dihydro-7-iodoindole

: 89976-15-8
7-iodo-1H-indole

Guidance literature:: With salcomine; oxygen; In methanol; for 4h;
DOI:10.1248/cpb.54.788

Reference yield: 70.0%

: 187099-51-0
tert-butyl (2-iodo-6-((trimethylsilyl)ethynyl)phenyl)carbamate

: 89976-15-8
7-iodo-1H-indole

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; for 8h; Heating;
DOI:10.3987/com-96-7636

Reference yield:

: 496-15-1
1-indoline

: 89976-15-8
7-iodo-1H-indole

Guidance literature:: Multi-step reaction with 4 steps

1.1: 94 percent / EDCI; pyridine / 24 h / 20 °C

2.1: trifluoroacetic acid; thallium trifluoroacetate / 24 h / 20 °C

2.2: 62 percent / aq. KI / 1 h / 20 °C

3.1: 91 percent / aq. NaOH / methanol / 0.5 h / 20 °C

4.1: 99 percent / salcomine; O₂ / methanol / 4 h

With pyridine; sodium hydroxide; salcomine; oxygen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; thallium(I) trifluoroacetate; trifluoroacetic acid; In methanol;
DOI:10.1248/cpb.54.788