(E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

Base Information

Chemical Name:(E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate
CAS No.:1365555-13-0
Molecular Formula:C₂₈H₂₉NO₅S
Molecular Weight:491.608
Hs Code.:

Synonyms:(E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

Suppliers and Price of (E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

There total 6 articles about (E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₁NO₅S

: 1365555-13-0
(E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1021/ja2109097

Reference yield:

: C₂₉H₃₇NO₄SSi

: 1365555-13-0
(E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

With dmap; tetrabutyl ammonium fluoride; Dess-Martin periodane; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja2109097

Reference yield:

: C₃₄H₄₅NO₅SSi

: 1365555-13-0
(E)-7-(N-(prop-2-ynyl)-N-tosylamino)-1-oxo-1-phenylhept-5-en-2-yn-4-yl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

With tetrabutyl ammonium fluoride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja2109097