C₁₉H₂₉NO₄

Base Information

Chemical Name:C₁₉H₂₉NO₄
CAS No.:1543007-23-3
Molecular Formula:C₁₉H₂₉NO₄
Molecular Weight:335.444
Hs Code.:

C<sub>19</sub>H<sub>29</sub>NO<sub>4</sub>

Synonyms:C₁₉H₂₉NO₄

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Chemical Property of C₁₉H₂₉NO₄

Chemical Property:

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Technology Process of C₁₉H₂₉NO₄

There total 13 articles about C₁₉H₂₉NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1543006-66-1
tert-butyl (2R,3S)-2-(2-(benzyloxy)ethyl)-3-((tert-butyldiphenylsilyloxy)methyl)pyrrolidine-1-carboxylate

: 1543007-23-3
C₁₉H₂₉NO₄

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 1543006-73-0
(2R,3S)-2-allyl-5-(benzyloxy)pentane-1,3-diol

: 1543007-23-3
C₁₉H₂₉NO₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: camphor-10-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 4 h / 20 °C / Inert atmosphere

3.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

5.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

6.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

7.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

8.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

9.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

10.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.2: 36 h / Inert atmosphere; Reflux

11.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; sodium azide; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; water; acetic acid; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 1543006-77-4
(4S,5R)-5-allyl-4-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxane

: 1543007-23-3
C₁₉H₂₉NO₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 4 h / 20 °C / Inert atmosphere

2.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

3.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

4.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

5.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

6.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

7.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

8.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

9.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

9.2: 36 h / Inert atmosphere; Reflux

10.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; sodium azide; tetrabutyl ammonium fluoride; water; acetic acid; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tet.2013.12.078