6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine

Base Information

• Chemical Name: 6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine
• CAS No.: 420834-63-5
• Molecular Formula: C₂₆H₂₄N₂O₃
• Molecular Weight: 412.488

Synonyms:6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine

Chemical Property of 6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine

Chemical Property:

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Technology Process of 6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine

There total 1 articles about 6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methylbenzonitrile (529-19-1) + 2,3,4-trimethoxybenzaldehyde (2103-57-3) → 6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine (420834-63-5)

Guidance literature:

With potassium tert-butylate; In various solvent(s); at 35 - 40 ℃;

DOI:10.1021/jm0490888

Reference yield:

6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine (420834-63-5) → 11-(2,3,4-trimethoxy-phenyl)-benzo[c]phenanthridin-6-ylamine

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; for 12h; Heating;

DOI:10.1021/jm0490888

Reference yield:

6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine (420834-63-5) → 11-(2,3,4-trimethoxy-phenyl)-11,12-dihydro-benzo[c]phenanthridin-6-ylamine + (R)-6-amino-11,12-dihydro-11-(2,3,4-trimethoxyphenyl)benzo[c]phenanthridine

Guidance literature:

chiral HPLC;

DOI:10.1021/jm0490888

upstream raw materials:

2-Methylbenzonitrile

2,3,4-trimethoxybenzaldehyde

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