[(2-benzoylpyridine)-3-isatin]bishydrazone

Base Information

• Chemical Name: [(2-benzoylpyridine)-3-isatin]bishydrazone
• CAS No.: 1555886-12-8
• Molecular Formula: C₂₀H₁₄N₄O
• Molecular Weight: 326.357
• Mol file: 1555886-12-8.mol

Synonyms:[(2-benzoylpyridine)-3-isatin]bishydrazone

Chemical Property of [(2-benzoylpyridine)-3-isatin]bishydrazone

Chemical Property:

Purity/Quality:

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Technology Process of [(2-benzoylpyridine)-3-isatin]bishydrazone

There total 1 articles about [(2-benzoylpyridine)-3-isatin]bishydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

phenyl(pyridin-2-yl)methanone (91-02-1) + 3-hydrazonoindolin-2-one (2365-44-8) → [(2-benzoylpyridine)-3-isatin]bishydrazone (1555886-12-8)

Guidance literature:

In methanol; Acidic conditions; Reflux;

DOI:10.1134/S1070363213120360

Reference yield: 70.0%

nickel(II) chloride hexahydrate + [(2-benzoylpyridine)-3-isatin]bishydrazone (1555886-12-8) + water (7732-18-5) → [Ni(bpish)(H2O)]Cl2*2H2O

Guidance literature:

In methanol; at 70 ℃; for 10h;

DOI:10.1002/kin.20861

Reference yield: 70.0%

nickel(II) chloride hexahydrate + [(2-benzoylpyridine)-3-isatin]bishydrazone (1555886-12-8) → [Ni(bpish)(H2O)]Cl2*2H2O

Guidance literature:

In methanol; water; at 70 ℃; for 10h; Thermodynamic data; Reflux;

DOI:10.1134/S1070363213120487

upstream raw materials:

phenyl(pyridin-2-yl)methanone

3-hydrazonoindolin-2-one