(S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE

Base Information

Chemical Name:(S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE
CAS No.:89959-26-2
Molecular Formula:C₆H₉BrN₂O₂
Molecular Weight:221.054
Hs Code.:
Mol file:89959-26-2.mol

Synonyms:(S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE

Suppliers and Price of (S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE 95.00%
5MG
$ 499.26

Total 4 raw suppliers

Chemical Property of (S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE

Chemical Property:

PSA：58.20000
LogP:0.04360

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

(S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE

There total 2 articles about (S)-3-(2-BROMOETHYL)-2,5-DIKETOPIPERAZINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 89959-25-1
3-L-(2-hydroxyethyl)diketopiperazine

: 89959-26-2
3-L-(2-bromoethyl)diketopiperazine

Guidance literature:: With bromine; triphenylphosphine; In N,N-dimethyl-formamide; 1) 0 deg C, 0.5 hr 2) 5 deg C;
DOI:10.1021/jo00186a042

Reference yield:

: 89959-29-5
N-(benzyloxycarbonyl)glycyl-L-homoserine lactone

: 89959-26-2
3-L-(2-bromoethyl)diketopiperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / H₂ / Pd-C / methanol / 18 h / 25 °C / 2068.6 Torr

2: 87 percent / triphenylphosphine, Br₂ / dimethylformamide / 1) 0 deg C, 0.5 hr 2) 5 deg C

With hydrogen; bromine; triphenylphosphine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00186a042

Reference yield:

: 89959-26-2
3-L-(2-bromoethyl)diketopiperazine

: 89975-16-6
Boc-L-Cys(Meb)-LL-Acp-OEt

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / CH₂Cl₂ / 18 h / 25 °C

2: 91 percent / Butyllithium / tetrahydrofuran / 3 h / -78 °C

3: 66 percent / 0.5 N HCl / 1 h / Ambient temperature

4: 82 percent / Ag₂O / H₂O; ethanol / 0.33 h

5: 85 percent / CH₂Cl₂ / 18 h / 5 °C

With hydrogenchloride; n-butyllithium; silver(l) oxide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jo00186a042