(S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]

Base Information

Chemical Name:(S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]
CAS No.:654667-04-6
Molecular Formula:C₄₁H₄₃N₃O₂
Molecular Weight:609.811
Hs Code.:

Synonyms:(S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]

Chemical Property:

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Technology Process of (S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]

There total 1 articles about (S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 22348-32-9,63401-04-7,112022-88-5,112068-01-6
(S)-diphenylprolinol

: 73004-40-7
2,6-bis-(bromomethyl)pyridine hydrobromide

: 654667-04-6
(S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]

Guidance literature:: With potassium carbonate; potassium iodide; In ethanol; at 20 ℃; for 8h;
DOI:10.1016/j.tetasy.2003.10.037

Reference yield: 83.0%

: iron(II) chloride

: 654667-04-6
(S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]

: [FeCl(2,6-bis[[(S)-2-(diphenylhydroxymethyl)-1-pyrrolidinyl]methyl]pyridine)]Cl

Guidance literature:: In methanol; dichloromethane; Schlenk techniques; soln. of FeCl2 (0.49 mmol) in dry MeOH added to soln. of org. ligand (0.49 mmol) in dry CH2Cl2; stirred (1 h, ambient temp.); evapd. (vac.); oil dissolved in min. amt. of dry MeOH; pptd. with dry Et2O; elem. anal.;
DOI:10.1016/j.ica.2006.08.009

Reference yield: 81.0%

: iron(II) trifluoromethanesulfonate acetonitrile disolvate

: 654667-04-6
(S,S)-1,1'-(2,6-pyridinyldimethyl)-bis[2-(diphenylmethanol)pyrrolidine]

: [Fe(OTf)(2,6-bis[[(S)-2-(diphenylhydroxymethyl)-1-pyrrolidinyl]methyl]pyridine)](OTf)

Guidance literature:: In dichloromethane; acetonitrile; Schlenk techniques; soln. of Fe(OTf)2*2MeCN (0.45 mmol) in MeCN added tosoln. of org. ligand (0.45 mmol) in dry CH2Cl2; stirred (1 h, ambient t emp.); evapd. (vac.); oil dissolved in min. amt. of dry MeOH; pptd. with dry Et2O; elem. anal.;
DOI:10.1016/j.ica.2006.08.009