C₅₉H₁₀₂O₉S₂Si₂

Base Information

Chemical Name:C₅₉H₁₀₂O₉S₂Si₂
CAS No.:930803-38-6
Molecular Formula:C₅₉H₁₀₂O₉S₂Si₂
Molecular Weight:1075.76
Hs Code.:

C<sub>59</sub>H<sub>102</sub>O<sub>9</sub>S<sub>2</sub>Si<sub>2</sub>

Synonyms:C₅₉H₁₀₂O₉S₂Si₂

Suppliers and Price of C₅₉H₁₀₂O₉S₂Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₉H₁₀₂O₉S₂Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₉H₁₀₂O₉S₂Si₂

There total 16 articles about C₅₉H₁₀₂O₉S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 930803-35-3
C₄₁H₆₆O₆S₂Si

: 156414-57-2
tert-Butyl-[(1R,2R,4S)-2-methoxy-4-((R)-(R)-2-oxiranyl-propyl)-cyclohexyloxy]-dimethyl-silane

: 930803-38-6
C₅₉H₁₀₂O₉S₂Si₂

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; at -78 - -40 ℃;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-26-2
C₉H₁₅S₂OBr

: 930803-38-6
C₅₉H₁₀₂O₉S₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

2: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

3: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

4: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

5: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; tert.-butyl lithium; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053

Reference yield:

: C₇H₁₂OS₂

: 930803-38-6
C₅₉H₁₀₂O₉S₂Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: potassium bis(trimethylsilyl)amide; [18]crown-6; bromine / tetrahydrofuran

2: 99 percent / diisobutylaluminum hydride / CH₂Cl₂ / -45 °C

3: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

4: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

5: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

6: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

7: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; 18-crown-6 ether; bromine; tert.-butyl lithium; potassium hexamethylsilazane; diisobutylaluminium hydride; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: Horner-Wadsworth-Emmons reaction;
DOI:10.1002/anie.200604053