Technology Process of C41H44O13
There total 18 articles about C41H44O13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
DOI:10.1021/ja00137a026
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 100 percent / DMAP, pyridine / 20 °C
2: 99 percent / H2 / 5percent Pd/C / ethanol / 20 °C
3: 1.) NBS, aq. HOAc, 2.) 70percent aq. HClO4 / 1.) 70 deg C, 2.) ethyl acetate, 0 deg C
4: 72 percent / benzene / 10 h / Heating
5: OsO4, NMO / acetone; H2O; 2-methyl-propan-2-ol
6: p-TSA
7: SiO2 / ethyl acetate
8: 100 percent / Dess-Martin periodinane / CH2Cl2 / 20 °C
With
pyridine; dmap; N-Bromosuccinimide; osmium(VIII) oxide; perchloric acid; N-methyl-2-indolinone; hydrogen; silica gel; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid;
palladium on activated charcoal;
In
ethanol; dichloromethane; water; ethyl acetate; acetone; tert-butyl alcohol; benzene;
DOI:10.1021/ja00137a026
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 99 percent / H2 / 5percent Pd/C / ethanol / 20 °C
2: 1.) NBS, aq. HOAc, 2.) 70percent aq. HClO4 / 1.) 70 deg C, 2.) ethyl acetate, 0 deg C
3: 72 percent / benzene / 10 h / Heating
4: OsO4, NMO / acetone; H2O; 2-methyl-propan-2-ol
5: p-TSA
6: SiO2 / ethyl acetate
7: 100 percent / Dess-Martin periodinane / CH2Cl2 / 20 °C
With
N-Bromosuccinimide; osmium(VIII) oxide; perchloric acid; N-methyl-2-indolinone; hydrogen; silica gel; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid;
palladium on activated charcoal;
In
ethanol; dichloromethane; water; ethyl acetate; acetone; tert-butyl alcohol; benzene;
DOI:10.1021/ja00137a026
