C₄₁H₅₄O₅

Base Information

• Chemical Name: C₄₁H₅₄O₅
• CAS No.: 1266102-56-0
• Molecular Formula: C₄₁H₅₄O₅
• Molecular Weight: 626.877
• Mol file: 1266102-56-0.mol

Synonyms:C₄₁H₅₄O₅

Chemical Property of C₄₁H₅₄O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₅₄O₅

There total 1 articles about C₄₁H₅₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

C41H56O4 (1246949-31-4) → C41H54O5 (1266102-56-0)

Guidance literature:

With boron trifluoride diethyl etherate; acetic acid; sodium nitrite; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo102054r

Reference yield: 86.0%

C41H54O5 (1266102-56-0) → C41H56O4 (1246949-31-4)

Guidance literature:

With hydrazine hydrate; potassium hydroxide; In ethylene glycol; Inert atmosphere;

DOI:10.1021/jo102054r

Reference yield:

C41H54O5 (1266102-56-0) → (3α,5α,11β,16β)-3,11-bis(benzyloxy)-16-hydroxypregnan-20-one (1246949-29-0)

Guidance literature:

Multi-step reaction with 6 steps

1: hydrazine hydrate; potassium hydroxide / ethylene glycol / Inert atmosphere

2: pyridine hydrochloride / 2 h / 135 °C / Inert atmosphere

3: chromium(VI) oxide; sodium acetate; acetic anhydride; acetic acid / water / 0.67 h / 0 °C / Inert atmosphere

4: aluminum oxide / benzene / 2.5 h / 20 °C / Inert atmosphere

5: water; N-bromoacetamide / tetrahydrofuran; acetone / 28 h / 20 °C / Inert atmosphere; Darkness

6: triethyl borane; tri-n-butyl-tin hydride / hexane; dichloromethane / 0.58 h / 20 °C / Inert atmosphere; In air

With chromium(VI) oxide; aluminum oxide; triethyl borane; water; tri-n-butyl-tin hydride; sodium acetate; pyridine hydrochloride; acetic anhydride; hydrazine hydrate; acetic acid; potassium hydroxide; N-bromoacetamide; In tetrahydrofuran; hexane; dichloromethane; water; ethylene glycol; acetone; benzene; 1: Wolff-Kishner reduction / 2: Marker's degradation;

DOI:10.1021/jo102054r

upstream raw materials:

C₄₁H₅₆O₄

Downstream raw materials:

C₄₁H₅₆O₄

C₄₃H₅₈O₅

(3α,5α,11β,16β)-3,11-bis(benzyloxy)-16-hydroxypregnan-20-one

C₄₇H₆₆O₆