benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate

Base Information

Chemical Name:benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate
CAS No.:1034763-75-1
Molecular Formula:C₂₂H₂₇N₃O₄S
Molecular Weight:429.54
Hs Code.:

Synonyms:benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate

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Chemical Property of benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate

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Technology Process of benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate

There total 1 articles about benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925244-55-9
benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl](2-oxoethyl)carbamate

: 75-31-0
isopropylamine

: 1034763-75-1
benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate

Guidance literature:: benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl](2-oxoethyl)carbamate; isopropylamine; In tetrahydrofuran; water; for 0.25h;

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; water; for 2h;

With water; sodium hydrogencarbonate; In tetrahydrofuran;

Reference yield:

: 1034763-76-2
N-[(benzyloxy)carbonyl]-N-(2-phenylethyl)-β-alanine

: 1034763-75-1
benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate

: 76-05-1
trifluoroacetic acid

: N1-(2-{[2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl]amino}ethyl)-N1-isopropyl-N3-(2-phenylethyl)-β-alaninamide bis-trifluoroacetate

Guidance literature:: N-[(benzyloxy)carbonyl]-N-(2-phenylethyl)-β-alanine; benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate; With N-ethyl-N,N-diisopropylamine; HATU; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 20h;

With ammonia; In methanol; for 0.5h;

trifluoroacetic acid; With hydrogen bromide; acetic acid; more than 3 stages;

Reference yield:

: 1034763-77-3
N-[(benzyloxy)carbonyl]-N-[2-(4-chlorophenyl)ethyl]-β-alanine

: 1034763-75-1
benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate

: 76-05-1
trifluoroacetic acid

: N3-[2-(4-chlorophenyl)ethyl]-N1-(2-{[2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl]amino}ethyl)-N1-isopropyl-β-alaninamide bis-trifluoroacetate

Guidance literature:: N-[(benzyloxy)carbonyl]-N-[2-(4-chlorophenyl)ethyl]-β-alanine; benzyl [2-(4-hydroxy-2-oxo-2,3-dihydro-1,3-benzothiazol-7-yl)ethyl][2-(isopropylamino)ethyl]carbamate; With N-ethyl-N,N-diisopropylamine; HATU; In 1-methyl-pyrrolidin-2-one; at 50 ℃; for 20h;

With ammonia; water; at 20 ℃; for 0.166667h;

trifluoroacetic acid; With hydrogen bromide; acetic acid; more than 3 stages;