2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester

Base Information

Chemical Name:2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester
CAS No.:155392-18-0
Molecular Formula:C₂₄H₂₈N₂O₃
Molecular Weight:392.498
Hs Code.:

Synonyms:2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester

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Chemical Property of 2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester

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Technology Process of 2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester

There total 3 articles about 2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 4442-88-0
1-phenyl-2-cyclohexylethylamine

: 1026946-77-9
2-Chloro-benzooxazole-5-carboxylic acid ethyl ester

: 155392-18-0
2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 24h; Heating;
DOI:10.1021/jm00033a008

Reference yield:

: 162959-44-6
5-ethoxycarbonyl-2-mercaptobenzoxazole

: 155392-18-0
2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃, PCl₅ / CH₂Cl₂ / 1 h / Ambient temperature

2: 66 percent / diisopropylethylamine / CH₂Cl₂ / 24 h / Heating

With phosphorus pentachloride; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In dichloromethane;
DOI:10.1021/jm00033a008

Reference yield:

: 13052-92-1
ethyl 3-amino-4-hydroxybenzoate

: 155392-18-0
2-<(2-cyclohexyl-1-phenylethyl)amino>-5-benzoxazolecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / methanol; H₂O

2: POCl₃, PCl₅ / CH₂Cl₂ / 1 h / Ambient temperature

3: 66 percent / diisopropylethylamine / CH₂Cl₂ / 24 h / Heating

With potassium hydroxide; phosphorus pentachloride; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In methanol; dichloromethane; water;
DOI:10.1021/jm00033a008