1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose

Base Information

Chemical Name:1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose
CAS No.:1030358-77-0
Molecular Formula:C₃₁H₃₅FO₆SSi
Molecular Weight:582.765
Hs Code.:

Synonyms:1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose

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Technology Process of 1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose

There total 1 articles about 1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1030358-76-9
1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-sulfinyl-D-ribitol

: 108-24-7
acetic anhydride

: 1030358-77-0
1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose

Guidance literature:: for 0.666667h; Heating;
DOI:10.1016/j.tet.2008.02.071

Reference yield: 77.0%

: 1030358-77-0
1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose

: 10457-14-4
O,O'-bis-(trimethylsilyl)uracil

: 1030358-78-1
C₃₃H₃₅FN₂O₆SSi

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In acetonitrile;
DOI:10.1016/j.tet.2008.02.071

Reference yield: 39.0%

: 1030358-77-0
1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose

: 87-42-3,111055-92-6
6-chloro-7H-purine

: 1030358-80-5
6-chloro-7-[5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(4-methoxybenzoyl)-4-thio-α/β-D-ribofuranosyl]-7H-purine

: 1030358-81-6
6-chloro-9-[5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(4-methoxybenzoyl)-4-thio-α/β-D-ribofuranosyl]-9H-purine

Guidance literature:: 6-chloro-7H-purine; With 1,1,1,3,3,3-hexamethyl-disilazane; In acetonitrile; Heating;

1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2-deoxy-2-fluoro-3-O-(p-methoxybenzoyl)-4-thio-α/β-D-ribofuranose; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; for 16h; Further stages.; Heating;
DOI:10.1016/j.tet.2008.02.071