(E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz

Base Information

Chemical Name:(E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz
CAS No.:130149-10-9
Molecular Formula:C₆H₁₅N*C₁₆H₁₇N₅O₄
Molecular Weight:444.534
Hs Code.:

Synonyms:(E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz

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Chemical Property of (E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz

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Technology Process of (E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz

There total 3 articles about (E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 130148-81-1
3-Azido-2-cyan-3-(1-ethoxycarbonyl-2-phenylethylamino)acrylsaeure-methylester

: 121-44-8
triethylamine

: 130149-10-9
(E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz

Guidance literature:: In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 13063-44-0
3,3-Dichlor-2-cyanacrylsaeure-methylester

: 130149-10-9
(E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / NaN₃ / acetone; H₂O / -15 °C

2: 86 percent / CH₂Cl₂ / 16 h / -30 °C

3: 99 percent / CH₂Cl₂ / 3 h / Ambient temperature

With sodium azide; In dichloromethane; water; acetone;

Reference yield:

: 82140-87-2
3,3-Diazido-2-cyan-acrylsaeure-methylester

: 130149-10-9
(E)-2-Cyan-2-<1-(1-ethoxycarbonyl)-2-phenylethyl)-4,5-dihydro-1H-tetrazol-5-yliden>essigsaeure-methylester, Triethylammonium-Salz

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / CH₂Cl₂ / 16 h / -30 °C

2: 99 percent / CH₂Cl₂ / 3 h / Ambient temperature

In dichloromethane;