3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran

Base Information

Chemical Name:3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran
CAS No.:1357077-04-3
Molecular Formula:C₁₆H₁₉NO₆
Molecular Weight:321.33
Hs Code.:

Synonyms:3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran

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Chemical Property of 3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran

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Technology Process of 3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran

There total 1 articles about 3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 1357077-22-5
3-acetyl-3-[(4-nitrophenyl)methyl]heptane-2,6-dione

: 1357077-04-3
3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran

: 4-[1,4-dimethyl-7-(4-nitrobenzyl)-2,3,5,6-tetraoxabicyclo[2.2.1]heptan-7-yl]butan-2-one

: 1-[(1R,2R,5S)-1,5-dimethyl-2-(4-nitrobenzyl)-6,7,8-trioxabicyclo[3.2.1]octan-2-yl]ethanone

: 1-[(1R,2S,5S)-1,5-dimethyl-2-(4-nitrobenzyl)-6,7,8-trioxabicyclo[3.2.1]octan-2-yl]ethanone

Guidance literature:: With phosphomolybdic acid; dihydrogen peroxide; In diethyl ether; toluene; at 20 - 25 ℃; for 8h; Green chemistry;
DOI:10.1134/S1070428015120027

Reference yield:

: 1357077-04-3
3,6,7a-trimethyl-3a-(4-nitrobenzyl)tetrahydro-3H,4H-3,6-epoxy[1,2]dioxolo[3,4-b]pyran

: 3-hydroxy-3-(4-nitrobenzyl)heptane-2,6-dione

: 1-(5-hydroxy-5-methyl-2-((4-nitrophenyl)methyl)tetrahydro-2-furanyl)ethanone

Guidance literature:: With ferrous(II) sulfate heptahydrate; sulfuric acid; In water; acetonitrile; at 20 - 25 ℃; for 1h; Overall yield = 75 %; Overall yield = 196 mg;
DOI:10.1016/j.tet.2016.04.054