3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester

Base Information

• Chemical Name: 3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester
• CAS No.: 847347-56-2
• Molecular Formula: C₂₈H₂₉BrO₅
• Molecular Weight: 525.439

Synonyms:3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester

Chemical Property of 3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester

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Technology Process of 3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester

There total 1 articles about 3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

C16H24O6S (847347-37-9) + 5-bromo-2-hydroxybenzophenone (55082-33-2) → 3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester (847347-56-2)

Guidance literature:

With caesium carbonate; In DMF (N,N-dimethyl-formamide); at 50 ℃; for 17h;

Reference yield: 100.0%

3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester (847347-56-2) → C27H26BrO5(1-)*Na(1+)

Guidance literature:

With methanol; sodium hydroxide; water; at 20 ℃;

Reference yield: 54.0%

3-{4-[3-(2-benzoyl-4-bromo-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester (847347-56-2) + butylboronic acid (4426-47-5) → 3-{4-[3-(2-benzoyl-4-butyl-phenoxy)-butoxy]-2-methyl-phenyl}-propionic acid methyl ester

Guidance literature:

With cesium fluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 80 ℃; for 10h;

upstream raw materials:

C₁₆H₂₄O₆S

5-bromo-2-hydroxybenzophenone

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