4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde

Base Information

Chemical Name:4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde
CAS No.:1333501-27-1
Molecular Formula:C₂₇H₄₄N₂O₃
Molecular Weight:444.658
Hs Code.:

Synonyms:4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde

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Chemical Property of 4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde

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Technology Process of 4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde

There total 1 articles about 4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 947769-95-1
4-(1-bromo-2-methylpropyl)-benzaldehyde

: 264280-22-0
4-tert-butyl-2,2,6,6-tetraethyl-3-oxo-piperazin-1-oxyl radical

: 1333501-27-1
4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde

Guidance literature:: With copper(II) trifluoroacetate; copper; 4,4'-di-tert-butyl-2,2'-bipyridine; In benzene; at 55 ℃; for 18h; Inert atmosphere;
DOI:10.1002/chem.201100543

Reference yield: 68.0%

: 1333501-27-1
4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde

: 1333501-28-2
1-tert-butyl-3,3,5,5-tetraethyl-4-(1-(4-(hydroxymethyl)phenyl)-2-methylpropoxy)piperazine-2-one

Guidance literature:: With sodium tetrahydroborate; In methanol; acetic acid; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201100543

Reference yield:

: 1333501-27-1
4-(1-(4-tert-butyl-2,2,6,6-tetraethyl-3-oxopiperazine-1-yloxy)-2-methylpropyl)benzaldehyde

: 1333501-29-3
1-(tert-butyl)-3,3,5,5-tetraethyl-4-(1-(4-(iodomethyl)phenyl)-2-methylpropoxy)piperazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol; acetic acid / 1 h / 0 - 20 °C / Inert atmosphere

2: chloro-trimethyl-silane; sodium iodide / acetonitrile / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; chloro-trimethyl-silane; sodium iodide; In methanol; acetic acid; acetonitrile;
DOI:10.1002/chem.201100543