Technology Process of C20H28N2O7
There total 6 articles about C20H28N2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H27NO7;
With
chloroformic acid ethyl ester; triethylamine;
In
tetrahydrofuran;
for 0.5h;
Inert atmosphere;
With
hydroxylamine hydrochloride; sodium methylate;
In
tetrahydrofuran; methanol;
for 24h;
DOI:10.1039/b916715c
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: piperidine; benzoic acid / ethanol / 5 h / Reflux
2.1: sodium cyanoborohydride / methanol / 20 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
4.1: tetrahydrofuran / 20 °C / Inert atmosphere
5.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h
5.2: 24 h
With
piperidine; hydrogen; chloroformic acid ethyl ester; sodium cyanoborohydride; triethylamine; benzoic acid;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; ethanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
2.1: tetrahydrofuran / 20 °C / Inert atmosphere
3.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h
3.2: 24 h
With
hydrogen; chloroformic acid ethyl ester; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol;
