N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide

Base Information

Chemical Name:N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide
CAS No.:1311285-48-9
Molecular Formula:C₂₀H₂₁N₃O₃S₂
Molecular Weight:415.537
Hs Code.:

Synonyms:N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide

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Chemical Property of N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide

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Technology Process of N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide

There total 4 articles about N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1220708-87-1
4-(5-(butylamino)-1,3,4-thiadiazol-2-yl)benzaldehyde

: 1939-99-7
benzenesulfonyl chloride

: 1311285-48-9
N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide

Guidance literature:: 4-(5-(butylamino)-1,3,4-thiadiazol-2-yl)benzaldehyde; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

benzenesulfonyl chloride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

Reference yield:

: 592-82-5
butyl isothiocyanate

: 1311285-48-9
N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / methanol / 1 h / 10 - 15 °C

2.1: trichlorophosphate / 1,4-dioxane / 1 h / 90 °C

2.2: 20 - 100 °C

3.1: osmium(VIII) oxide; sodium periodate / water; acetone / 3 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; hydrazine hydrate; sodium hydride; trichlorophosphate; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 6610-31-7
4-butyl-3-thiosemicarbazide

: 1311285-48-9
N-butyl-N-[5-(4-formylphenyl)-1,3,4-thiadiazol-2-yl]-1-phenylmethanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 1,4-dioxane / 1 h / 90 °C

1.2: 20 - 100 °C

2.1: osmium(VIII) oxide; sodium periodate / water; acetone / 3 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; sodium hydride; trichlorophosphate; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetone;