(S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate

Base Information

• Chemical Name: (S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate
• CAS No.: 956569-92-9
• Molecular Formula: C₂₂H₂₀N₂O₆
• Molecular Weight: 408.411

Synonyms:(S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate

Chemical Property of (S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate

Chemical Property:

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Technology Process of (S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate

There total 1 articles about (S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6) + 7-(1H-benzo[d][1,2,3]triazole-1-carbonyl)-5-ethyl-[1,3]dioxolo[4,5-g]quinolin-8(5H)-one (1131147-59-5) → (S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate (956569-92-9)

Guidance literature:

With triethylamine; In water; acetonitrile; at 20 ℃; for 3h;

DOI:10.1039/b900762h

Reference yield: 89.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + (S)-2-(5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamido)-3-phenylpropanoate (956569-92-9) → (S)-N-(1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-yl)-5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamide (1381762-73-7)

Guidance literature:

With thionyl chloride; In dichloromethane; at -15 ℃; for 4.5h;

DOI:10.1039/c2ob26439k

upstream raw materials:

L-phenylalanine

7-(1H-benzo[d][1,2,3]triazole-1-carbonyl)-5-ethyl-[1,3]dioxolo[4,5-g]quinolin-8(5H)-one

Downstream raw materials:

(S)-N-(1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-phenylpropan-2-yl)-5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinoline-7-carboxamide

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