5-(cyclohexylamino)-2,2-diethyl-4-methoxy-1-oxonia-2-borata-3,5-cyclopentadiene

Base Information

Chemical Name:5-(cyclohexylamino)-2,2-diethyl-4-methoxy-1-oxonia-2-borata-3,5-cyclopentadiene
CAS No.:105858-56-8
Molecular Formula:C₁₄H₂₆BNO₂
Molecular Weight:251.177
Hs Code.:

Synonyms:5-(cyclohexylamino)-2,2-diethyl-4-methoxy-1-oxonia-2-borata-3,5-cyclopentadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(cyclohexylamino)-2,2-diethyl-4-methoxy-1-oxonia-2-borata-3,5-cyclopentadiene

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Technology Process of 5-(cyclohexylamino)-2,2-diethyl-4-methoxy-1-oxonia-2-borata-3,5-cyclopentadiene

There total 1 articles about 5-(cyclohexylamino)-2,2-diethyl-4-methoxy-1-oxonia-2-borata-3,5-cyclopentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 97-94-9
triethyl borane

: 594-19-4
tert.-butyl lithium

: 98083-80-8
2-Methoxy-propensaeure-N-cyclohexylamid

: 105858-56-8
5-(cyclohexylamino)-2,2-diethyl-4-methoxy-1-oxonia-2-borata-3,5-cyclopentadiene

Guidance literature:: In tetrahydrofuran; hexane; prepn. the N-Li compd.in THF, addn. of BEt3 in hexane under N2 at -80°C and stirring for 0.5 h; pouring into water, acidifying to pH 1 (1N HCl), extn. with CH2Cl2, drying (Na2SO4), evapn. (vac.), flash chromy. on silica gel and elution with petroleum ether-ethyl acetate; elem. anal.;