Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3

Base Information

Chemical Name:Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3
CAS No.:155019-73-1
Molecular Formula:C₃₃H₃₃F₁₅MoN₆Si
Molecular Weight:922.667
Hs Code.:

Mo(N(CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)3)NNSi(CH(CH<sub>3</sub>)2)3

Synonyms:Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3

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Chemical Property of Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3

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Technology Process of Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3

There total 2 articles about Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 155019-65-1
((C₆F₅NCH₂CH₂)3N)MoOTf

: 13154-24-0
triisopropylsilyl chloride

: 155019-73-1
Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3

Guidance literature:: With Na#Hg; N₂; In tetrahydrofuran; under N2; the Mo complex was added to sodium amalgam in THF, stirred for 10 min, filtered, cooled to -35°C, addn. of the silyl chloride, stirred for 10 min; solvent was removed in vac., extd. with pentane, pentane was removed in vac., recrystd. by slow diffusion of pentane into a ether soln.; elem. anal.;
DOI:10.1021/ja00089a028

Reference yield:

: 2Mo⁽³⁺⁾*2N(CH₂CH₂NC₆F₅)3^(3-)*⁽¹⁵⁾N₂={Mo₂(N(CH₂CH₂NC₆F₅)3)2(⁽¹⁵⁾N₂)}

: 155019-73-1
Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3

: 155019-76-4
Mo(N(CH₂CH₂NC₆F₅)3)⁽¹⁵⁾N⁽¹⁵⁾NSi(CH(CH₃)2)3

Guidance literature:: With Na#Hg; In tetrahydrofuran; the Mo complex was added to sodium amalgam in THF, stirred at 25°C for 25 min, addn. of the silyl chloride; solvent was removed in vac., extd. with pentane, pentane was removed in vac., washed with pentane, dried in vac. (mixt. of the two compds.);
DOI:10.1021/ja00089a028

Reference yield:

: 155019-73-1
Mo(N(CH₂CH₂NC₆F₅)3)NNSi(CH(CH₃)2)3

: 155019-65-1
((C₆F₅NCH₂CH₂)3N)MoOTf

Guidance literature:: With ferrocenium triflate; In dichloromethane; under exclusion of air; a soln. the triflate in CH2Cl2 was added to a soln. of the Mo complex; product was washed with CH2Cl2, dried in vac.;
DOI:10.1021/ja00089a028