C₄₁H₅₇NO₉Si

Base Information

Chemical Name:C₄₁H₅₇NO₉Si
CAS No.:1446749-27-4
Molecular Formula:C₄₁H₅₇NO₉Si
Molecular Weight:735.99
Hs Code.:

C<sub>41</sub>H<sub>57</sub>NO<sub>9</sub>Si

Synonyms:C₄₁H₅₇NO₉Si

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Chemical Property of C₄₁H₅₇NO₉Si

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Technology Process of C₄₁H₅₇NO₉Si

There total 10 articles about C₄₁H₅₇NO₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1446749-26-3
C₄₄H₆₁NO₉Si

: 1446749-27-4
C₄₁H₅₇NO₉Si

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1002/chem.201204550

Reference yield:

: 1446749-05-8
C₂₇H₄₅N₃O₁₁Si

: 1446749-27-4
C₄₁H₅₇NO₉Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C

1.2: IR-120 resin

2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

2.2: 2 h / 0 - 20 °C

3.1: triphenylphosphine / tetrahydrofuran; water / 12 h / 20 °C

4.1: pyridine / 12 h / 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

With pyridine; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204550

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 1446749-27-4
C₄₁H₅₇NO₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Molecular sieve

2.1: trifluoroacetic acid; trifluoroacetic anhydride / dichloromethane / 0.5 h / 0 °C

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Molecular sieve; Inert atmosphere

4.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C

4.2: IR-120 resin

5.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

5.2: 2 h / 0 - 20 °C

6.1: triphenylphosphine / tetrahydrofuran; water / 12 h / 20 °C

7.1: pyridine / 12 h / 0 - 20 °C

8.1: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

With pyridine; 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204550