ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate

Base Information

Chemical Name:ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate
CAS No.:1254254-10-8
Molecular Formula:C₁₈H₂₅N₃O₆
Molecular Weight:379.413
Hs Code.:

Synonyms:ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate

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Chemical Property of ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate

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Technology Process of ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate

There total 5 articles about ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1060639-85-1
ethyl 1-isocyanato-2,2-dimethylcyclopropanecarboxylate

: 41764-74-3
3,4-dimethoxybenzohydrazide

: 1254254-10-8
ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate

Guidance literature:: at 20 ℃;
DOI:10.1016/j.ejmech.2012.05.037

Reference yield:

: C₁₂H₁₈O₆

: 1254254-10-8
ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / tetrahydrofuran; water / 1 h / -15 - -10 °C

2: toluene / 75 °C

3: 20 °C

With sodium azide; In tetrahydrofuran; water; toluene; 2: Curtius rearrangement;
DOI:10.1016/j.ejmech.2012.05.037

Reference yield:

: 859689-01-3
1-(ethoxycarbonyl)-2,2-dimethylcyclopropanecarboxylic acid

: 1254254-10-8
ethyl 1-(2-(3,4-dimethoxybenzoyl)hydrazinecarboxamido)-2,2-dimethylcyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methyl-morpholine / tetrahydrofuran / 0.33 h / -15 °C

2: sodium azide / tetrahydrofuran; water / 1 h / -15 - -10 °C

3: toluene / 75 °C

4: 20 °C

With 4-methyl-morpholine; sodium azide; In tetrahydrofuran; water; toluene; 3: Curtius rearrangement;
DOI:10.1016/j.ejmech.2012.05.037