C₁₄H₁₄ClF₂NO₂

Base Information

Chemical Name:C₁₄H₁₄ClF₂NO₂
CAS No.:1292820-62-2
Molecular Formula:C₁₄H₁₄ClF₂NO₂
Molecular Weight:301.72
Hs Code.:

C<sub>14</sub>H<sub>14</sub>ClF<sub>2</sub>NO<sub>2</sub>

Synonyms:C₁₄H₁₄ClF₂NO₂

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Chemical Property of C₁₄H₁₄ClF₂NO₂

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Technology Process of C₁₄H₁₄ClF₂NO₂

There total 2 articles about C₁₄H₁₄ClF₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 61550-02-5
(furan-2-yloxy)-trimethylsilane

: 1292820-53-1
C₁₀H₁₀ClF₂N

: 1292820-62-2
C₁₄H₁₄ClF₂NO₂

Guidance literature:: (furan-2-yloxy)-trimethylsilane; C₁₀H₁₀ClF₂N; With ethanol; silver(I) acetate; (aS)-tBu-BinaphPHOX; In tetrahydrofuran; at -78 ℃; for 7h; Molecular sieve;

With acetic acid; In tetrahydrofuran; methanol; at -78 ℃; for 2h; enantioselective reaction;
DOI:10.1002/adsc.201000843

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1292820-62-2
C₁₄H₁₄ClF₂NO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / Reflux

2.1: ethanol; silver(I) acetate; (aS)-tBu-BinaphPHOX / tetrahydrofuran / 7 h / -78 °C / Molecular sieve

2.2: 2 h / -78 °C

With ethanol; silver(I) acetate; (aS)-tBu-BinaphPHOX; In tetrahydrofuran; toluene; 2.1: Mannich type reaction;
DOI:10.1002/adsc.201000843

Reference yield:

: 1292820-62-2
C₁₄H₁₄ClF₂NO₂

: 1292820-72-4
C₁₃H₁₁BrClF₂NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium(II) hydroxide / methanol / 7 h / 22 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 22 °C

With hydrogen; palladium(II) hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201000843