2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate

Base Information

Chemical Name:2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate
CAS No.:1094039-30-1
Molecular Formula:C₄₀H₅₁NO₄SSi
Molecular Weight:670.001
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate

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Chemical Property of 2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate

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Technology Process of 2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate

There total 1 articles about 2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 1094039-27-6
(S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoic acid

: 1094039-30-1
2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 14h; Inert atmosphere; Cooling with ice;
DOI:10.1021/jo802415c

Reference yield: 87.0%

: 1094039-30-1
2-(trimethylsilyl)ethyl (S)-2-(1-(4,4-dimethyl-2,6-dioxocyclohexylidene)-3-methylbutylamino)-3-(tritylthio)-propanoate

: 1094039-31-2
C₂₁H₃₇NO₄SSi

Guidance literature:: With chlorotriisopropylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Cooling with ice;
DOI:10.1021/jo802415c