4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside
CAS No.:1107660-59-2
Molecular Formula:C₄₂H₄₃NO₆S
Molecular Weight:689.873
Hs Code.:

Synonyms:4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

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Chemical Property of 4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

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Technology Process of 4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

There total 3 articles about 4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 16766-09-9
(4-acetamidophenyl)disulfide

: (2,3,4,6-tetra-O-benzyl-2-β-D-glucopyranosyl)tri-n-butylstannane

: 1107660-59-2
4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: With copper(l) chloride; In 1,2-dichloro-ethane; m-xylene; at 130 ℃; for 96h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jacs.8b11211

Reference yield:

: 1107660-57-0
C₄₀H₄₁NO₅S

: 108-24-7
acetic anhydride

: 1107660-59-2
4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; In ethanol; dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/b813048e

Reference yield:

: 1126-81-4
4-acetamidothiophenol

: 1107660-59-2
4-(acetylamino)phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium perborate; acetic acid / water / 4 h / 20 °C

2: copper(l) chloride / m-xylene; 1,2-dichloro-ethane / 96 h / 130 °C / Inert atmosphere

With sodium perborate; acetic acid; copper(l) chloride; In water; 1,2-dichloro-ethane; m-xylene;
DOI:10.1021/jacs.8b11211