2-benzyl-3-aza-5-hexenyl phenyl selenide

Base Information

Chemical Name:2-benzyl-3-aza-5-hexenyl phenyl selenide
CAS No.:281669-88-3
Molecular Formula:C₁₈H₂₁NSe
Molecular Weight:330.331
Hs Code.:

Synonyms:2-benzyl-3-aza-5-hexenyl phenyl selenide

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Chemical Property of 2-benzyl-3-aza-5-hexenyl phenyl selenide

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Technology Process of 2-benzyl-3-aza-5-hexenyl phenyl selenide

There total 2 articles about 2-benzyl-3-aza-5-hexenyl phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1666-13-3
diphenyl diselenide

: 281669-83-8
N-allyl-2-benzyl-aziridine

: 281669-88-3
2-benzyl-3-aza-5-hexenyl phenyl selenide

Guidance literature:: diphenyl diselenide; With sodium tetrahydroborate; In tetrahydrofuran; water;

N-allyl-2-benzyl-aziridine; With trifluoroacetic acid; In tetrahydrofuran; water; for 1h; Further stages.;
DOI:10.1021/ol005829x

Reference yield:

: 13906-90-6
2-benzylaziridine

: 281669-88-3
2-benzyl-3-aza-5-hexenyl phenyl selenide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -78 °C

1.2: 84 percent / tetrahydrofuran; hexane / -78 - 20 °C

2.1: NaBH₄ / tetrahydrofuran; H₂O

2.2: 86 percent / TFA / tetrahydrofuran; H₂O / 1 h

With sodium tetrahydroborate; n-butyllithium; In tetrahydrofuran; hexane; water; 1.1: Metallation / 1.2: Addition / 2.1: Reduction / 2.2: Ring cleavage;
DOI:10.1021/ol005829x