11-bromo-undecanoic acid (2-formyl-phenyl)-amide

Base Information

• Chemical Name: 11-bromo-undecanoic acid (2-formyl-phenyl)-amide
• CAS No.: 240813-39-2
• Molecular Formula: C₁₈H₂₆BrNO₂
• Molecular Weight: 368.314
• Mol file: 240813-39-2.mol

Synonyms:11-bromo-undecanoic acid (2-formyl-phenyl)-amide

Chemical Property of 11-bromo-undecanoic acid (2-formyl-phenyl)-amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 11-bromo-undecanoic acid (2-formyl-phenyl)-amide

There total 4 articles about 11-bromo-undecanoic acid (2-formyl-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

11-bromo-undecanoic acid [2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenyl]-amide → 11-bromo-undecanoic acid (2-formyl-phenyl)-amide (240813-39-2)

Guidance literature:

With sulfuric acid; trifluoroacetic acid;

DOI:10.1039/a809918i

Reference yield:

5,5-Dimethyl-2-(2-nitro-phenyl)-[1,3]dioxane (79718-94-8) → 11-bromo-undecanoic acid (2-formyl-phenyl)-amide (240813-39-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 72 percent / H₂ / Pd/C

2: 99 percent / N-methylmorpholine, 2-chloro-4,6-dimethoxy-1,3,5-triazine

3: 99 percent / H₂SO₄, TFA

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sulfuric acid; hydrogen; trifluoroacetic acid; palladium on activated charcoal;

DOI:10.1039/a809918i

Reference yield:

2-nitro-benzaldehyde (552-89-6) → 11-bromo-undecanoic acid (2-formyl-phenyl)-amide (240813-39-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / TsOH

2: 72 percent / H₂ / Pd/C

3: 99 percent / N-methylmorpholine, 2-chloro-4,6-dimethoxy-1,3,5-triazine

4: 99 percent / H₂SO₄, TFA

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sulfuric acid; hydrogen; toluene-4-sulfonic acid; trifluoroacetic acid; palladium on activated charcoal;

DOI:10.1039/a809918i

upstream raw materials:

5,5-Dimethyl-2-(2-nitro-phenyl)-[1,3]dioxane

2-nitro-benzaldehyde

2-(5,5-dimethyl-[1,3]dioxan-2-yl)-phenylamine

Downstream raw materials:

thioacetic acid S-[10-(2-formyl-phenylcarbamoyl)-decyl] ester

11-mercapto-undecanoic acid (2-formyl-phenyl)-amide