N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide

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Chemical Name:N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide
CAS No.:1039756-17-6
Molecular Formula:C₂₅H₃₂N₂O₄S
Molecular Weight:456.606
Hs Code.:

Synonyms:N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide

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Chemical Property of N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide

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Technology Process of N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide

There total 3 articles about N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 960054-45-9
N-mesitylenesulfonyl aziridine

: 1039756-01-8
N-(tert-butyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxamide

: 1039756-17-6
N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide

Guidance literature:: With 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; In tetrahydrofuran; at 25 ℃; for 48.1667h;
DOI:10.1039/b802447b

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 1039756-17-6
N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / -10 - 20 °C / Inert atmosphere

2.1: potassium hydroxide / water; toluene / 25 °C / Inert atmosphere

3.1: 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine / tetrahydrofuran / 0.17 h / 25 °C / Inert atmosphere

3.2: 48 h / 25 °C / Inert atmosphere

With pyridine; 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; potassium hydroxide; In tetrahydrofuran; water; toluene;
DOI:10.1002/chem.201203825

Reference yield:

: 70823-23-3
2,4-(dimesitylsulfonyl)ethanolamine

: 1039756-17-6
N-(tert-butyl)-1-oxo-2-(2-(mesitylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / water; toluene / 25 °C / Inert atmosphere

2.1: 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine / tetrahydrofuran / 0.17 h / 25 °C / Inert atmosphere

2.2: 48 h / 25 °C / Inert atmosphere

With 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; potassium hydroxide; In tetrahydrofuran; water; toluene;
DOI:10.1002/chem.201203825