C₂₂H₂₂OSi

Base Information

• Chemical Name: C₂₂H₂₂OSi
• CAS No.: 1433962-62-9
• Molecular Formula: C₂₂H₂₂OSi
• Molecular Weight: 330.502
• Mol file: 1433962-62-9.mol

Synonyms:C₂₂H₂₂OSi

Chemical Property of C₂₂H₂₂OSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₂OSi

There total 2 articles about C₂₂H₂₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

ethyl (E)-1-phenylbut-1-en-3-ol (36004-04-3) → C22H22OSi (1433962-62-9)

Guidance literature:

ethyl (E)-1-phenylbut-1-en-3-ol; With diphenylsilyl chloride; triethylamine; In diethyl ether; at 0 ℃; for 0.333333h; Inert atmosphere; Cooling with ice;

In diethyl ether; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1039/c3dt32983f

Reference yield:

C22H21(2)HOSi (1433962-65-2) → C22H22OSi (1433962-62-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triazolylidene / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C / Inert atmosphere

2.1: diphenylsilyl chloride; triethylamine / diethyl ether / 0.33 h / 0 °C / Inert atmosphere; Cooling with ice

2.2: 18 h / 20 °C / Inert atmosphere

With triazolylidene; diphenylsilyl chloride; triethylamine; In diethyl ether; N,N-dimethyl-formamide;

DOI:10.1039/c3dt32983f

Reference yield: 75.0%

C22H22OSi (1433962-62-9) → C22H22OSi

Guidance literature:

C₂₂H₂₂OSi; In tetrahydrofuran; for 0.0833333h; Molecular sieve; Inert atmosphere;

With Wilkinson's catalyst; In tetrahydrofuran; for 4h; Molecular sieve; Inert atmosphere; Reflux;

DOI:10.1039/c3dt32983f

upstream raw materials:

C₂₂H₂₁⁽²⁾HOSi

ethyl (E)-1-phenylbut-1-en-3-ol

Downstream raw materials:

1-phenyl-3-butanol