benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate

Base Information

• Chemical Name: benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate
• CAS No.: 785827-87-4
• Molecular Formula: C₂₇H₂₅N₂O₅P
• Molecular Weight: 488.48
• Mol file: 785827-87-4.mol

Synonyms:benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate

Chemical Property of benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate

There total 5 articles about benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

diphenyl (benzyloxycarbonylamino)(m-nitrophenyl)methylphosphonate (169828-94-8) → benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate (785827-87-4)

Guidance literature:

With tin(ll) chloride; In water; ethyl acetate; Heating;

DOI:10.1016/j.tetlet.2004.08.021

Reference yield:

triphenyl phosphite (101-02-0) → benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate (785827-87-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / AcOH / 80 °C

2: 99 percent / SnCl₂ / H₂O; ethyl acetate / Heating

With acetic acid; tin(ll) chloride; In water; ethyl acetate;

DOI:10.1016/j.tetlet.2004.08.021

Reference yield:

O-benzyl carbamate (621-84-1) → benzyl ((3-aminophenyl)(diphenoxyphosphoryl)methyl)carbamate (785827-87-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / AcOH / 80 °C

2: 99 percent / SnCl₂ / H₂O; ethyl acetate / Heating

With acetic acid; tin(ll) chloride; In water; ethyl acetate;

DOI:10.1016/j.tetlet.2004.08.021

upstream raw materials:

diphenyl (benzyloxycarbonylamino)(m-nitrophenyl)methylphosphonate

triphenyl phosphite

O-benzyl carbamate

3-nitro-benzaldehyde

Downstream raw materials:

C₃₈H₄₃N₄O₉P